SOP for Micrometer | Pharmaguideline
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  • Apr 17, 2021

    SOP for Micrometer

    Standard operating procedure of Micrometer used in Quality Control.

    1.0 OBJECTIVE

    To describe the procedure for operation of Micrometer.

    2.0 SCOPE

    This SOP is applicable for operation of Micrometer.

    3.0 RESPONSIBILITY

    Officer/ Executive - Quality Control

    4.0 ACCOUNTABILITY

    Manager – Quality Control

    5.0 PROCEDURE

    5.1 Operating procedure

    5.1.1 Turn the thimble to gently bring the spindle in to contact with the anvil. Apply the rated measuring force using the ratchet stop/friction thimble.
    5.1.2 Press the zero buttons to zero setting display 0.0000 on the screen.
    5.1.3 To 0.0000 setting indicating the origin has been set.
    5.1.4 To set the required measurement value. Press IN/MM changeover buttons.
    5.1.5 Note the reading.

    5.2 Cleaning procedure

    5.2.1 Clean measuring jaws holding disks with a slightly wet cloth and then with a dry cotton cloth.
    5.2.2 Clean measuring jaws holding disks with a dry cotton cloth whenever required during and after the test.

    5.3 Calibration procedure

    5.3.1 Calibration of micrometer following standard calibrate equipment are as follows
              Standard slip gauge       Standard metal gauge block
              Asset No.                     -------------------         --------------------
              Make                           Mitutoyo                        Mitutoyo
              Capacity                       0.05mm to 1.00 mm      Width 25.00mm, length 34.90mm hight 8.9mm
              Location                       QC Laboratory              QC Laboratory
              Calibrated by -             External party                 External party
              Calibration frequency-  Once in two years.         Once in two years

    5.3.2 Calibration can be done in-house or by the external party.
    5.3.3 For micrometer press on key with the jaw closed.
    5.3.4 Ensure “zero”reading with the jaw closed.
    5.3.5 Open the jaw.
    5.3.6 Measure the thickness of standard slip gauge (0.05 mm to 1.00 mm) by putting individual gauge between the jaw.

    5.3.7 Note the observations in Annexure I. Annexure I is not applicable if the calibration is done by outside party.
    5.3.8 Measure the length, width and height standard metal gauge block (8.90 mm, 25 mm and 34.90 mm respectively) by putting the standard metal gauge block in between the jaws.
    5.3.9 Note the reading in Annexure I. Annexure I is not applicable if the calibration is done by outside party.
    5.3.10 Affix the calibration status label.
    5.3.11 Frequency of Calibration: Once in two years by the external party.
    5.3.12 If calibration is out of calibration then inform to head of the department for further action.

    6.0 ABBREVIATIONS

    6.1 SOP - Standard Operating Procedure
    6.2 No. - Number
    6.3 QA - Quality Assurance
    6.4 NA - Not Applicable
    6.5 CCF - Change control format
    6.6 QC - Quality Control


    ANNEXURE-I
    CALIBRATION OF MICROMETER
    Asset ID  No.
    :

    Ref.  SOP No.
    :

    Make
    :

    Model No.
    :

    Date:
    S.No
    Nominal size in mm (slip gauge)
    Tolerance in mm (±5% of nominal size in mm)
    Observed value in mm
    Calibrated by
    Checked by
    Remark
    1
    0.05
    0.048-0.052




    2
    0.10
    0.095-0.105




    3
    0.15
    0.143-0.157




    4
    0.20
    0.190-0.210




    5
    0.25
    0.240-0.260




    6
    0.30
    0.285-0.315




    7
    0.35
    0.340-0.360




    8
    0.40
    0.380-0.420




    9
    0.45
    0.430-0.470




    10
    0.50
    0.475-0.525




    11
    0.55
    0.530-0.570




    12
    0.60
    0.570-0.630




    13
    0.65
    0.620-0.680




    14
    0.70
    0.665-0.735




    15
    0.75
    0.720-0.780




    16
    0.80
    0.760-0.840




    17
    0.85
    0.810-0.890




    18
    0.90
    0.855-0.945




    19
    0.95
    0.910-0.990




    20
    1.00
    0.950-1.050




    Date :
    S.No.

    Nominal size standard metal gauge block mm
    Tolerance in mm
    Observed value in mm
    Calibrated by
    Checked by
    Remark
    1
    Width=25.00mm
    23.75-26.25




    2
    Length=34.90mm
    33.20-36.65




    3
    Height=8.90mm
    8.50-9.35




    Remark:  For micrometer least count 0.05mm use slip gauge measurement 0.20mm to 1.00mm and use metal gauge block.
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