Preparation and Standardization of 0.1 M Titanium Trichloride : Pharmaceutical Guidelines

Preparation and Standardization of 0.1 M Titanium Trichloride

Preparation and standardisation of 0.1 M Titanium Trichloride using 0.1 M ferric ammonium sulphate and ammonium thiocyanate solution as indicator.
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Titanium Trichloride Solution Preparation

  • Dilute 100 ml of titanium trichloride solution with 200 ml of hydrochloric acid.
  • Add sufficient freshly boiled and cooled water to produce 1000 ml.

Titanium Trichloride Solution Standardization

  • Standardize the solution immediately before use by titrating with it in an atmosphere of carbon dioxide.
  • Titrate 25 ml of 0.1 M ferric ammonium sulfate (acidified with sulphuric acid) with the 0.1 M Titanium Trichloride solution, using ammonium thiocyanate solution as indicator.
  • 1 ml of 0.1 M ferric ammonium sulfate is equivalent to 0.01543 g of TiCl3.
Also see: Determination of Shelf Life of Solutions in Laboratory

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Ankur Choudhary is India's first professional pharmaceutical blogger, author and founder of Pharmaceutical Guidelines, a widely-read pharmaceutical blog since 2008. Sign-up for the free email updates for your daily dose of pharmaceutical tips.
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